ASTM D3749-2008 用气相色谱液上技术测定聚氯乙烯树脂中残余氯乙烯单体的标准试验方法
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【英文标准名称】:StandardTestMethodforResidualVinylChlorideMonomerinPoly(VinylChloride)ResinsbyGasChromatographicHeadspaceTechnique
【原文标准名称】:用气相色谱液上技术测定聚氯乙烯树脂中残余氯乙烯单体的标准试验方法
【标准号】:ASTMD3749-2008
【标准状态】:现行
【国别】:美国
【发布日期】:2008
【实施或试行日期】:
【发布单位】:美国材料与试验协会(US-ASTM)
【起草单位】:D20.70
【标准类型】:(TestMethod)
【标准水平】:()
【中文主题词】:
【英文主题词】:gaschromatography;headspacegaschromatography;poly(vinylchloride);vinylchloridemonomer;Headspacegaschromatography;Poly(vinylchloride)(PVC)resins;Vinylchloridemonomercontent;Gaschromatography(GC)--plastics
【摘要】:Poly(vinylchloride)resinsmustcontainaminimumpossibleamountofunreacted,orfree,VCM.ThistestmethodprovidesameasureofRVCMwhichissuitableformanufacturingcontrolorspecificationacceptancepurposes.Underoptimumconditions,alowerlevelofdetectionof2ppmbyvolumeVCMcanbedetectedintheheadspacevapor.Usinga4-gsample,thisisequivalenttoabout0.02ppmbymassRVCMinthePVCresin.1.1Thistestmethodissuitablefordeterminingtheresidualvinylchloridemonomer(RVCM)contentofpoly(vinylchloride)(PVC)homopolymerandcopolymerresinsforusesotherthanfoodcontact.Therangeforthistest,basedoninterlaboratoryevaluation,isfrom0.1to400ppmRVCM.1.2ThistestmethodcanbeadaptedtodeterminationsofRVCMinaPVCcopolymerresiniftheHenry''sLawconstantat90x00B0;Cforthatcopolymerisknown.1.3Thistestmethodcannotbeusedforpolymerinfusedforms,suchascubesorsheets.RefertoTestMethodD4443orTestMethodD3680forthesematerials.1.4ThistestmethodisproposedasanalternativetoEPAMethod107fordeterminationofvinylchloridemonomersindry-resinsamples.1.5ThevaluesstatedSIunitsaretoberegardedasthestandard.1.6Thisstandarddoesnotpurporttoaddressallofthesafetyconcerns,ifany,associatedwithitsuse.Itistheresponsibilityoftheuserofthisstandardtoestablishappropriatesafetyandhealthpracticesanddeterminetheapplicabilityofregulatorylimitationspriortouse.Note18212;ThisstandardandISO6401:2008addressthesamesubjectmatter,butdifferintechnicalcontent.
【中国标准分类号】:G31
【国际标准分类号】:83_080_20
【页数】:4P.;A4
【正文语种】:英语
【原文标准名称】:用气相色谱液上技术测定聚氯乙烯树脂中残余氯乙烯单体的标准试验方法
【标准号】:ASTMD3749-2008
【标准状态】:现行
【国别】:美国
【发布日期】:2008
【实施或试行日期】:
【发布单位】:美国材料与试验协会(US-ASTM)
【起草单位】:D20.70
【标准类型】:(TestMethod)
【标准水平】:()
【中文主题词】:
【英文主题词】:gaschromatography;headspacegaschromatography;poly(vinylchloride);vinylchloridemonomer;Headspacegaschromatography;Poly(vinylchloride)(PVC)resins;Vinylchloridemonomercontent;Gaschromatography(GC)--plastics
【摘要】:Poly(vinylchloride)resinsmustcontainaminimumpossibleamountofunreacted,orfree,VCM.ThistestmethodprovidesameasureofRVCMwhichissuitableformanufacturingcontrolorspecificationacceptancepurposes.Underoptimumconditions,alowerlevelofdetectionof2ppmbyvolumeVCMcanbedetectedintheheadspacevapor.Usinga4-gsample,thisisequivalenttoabout0.02ppmbymassRVCMinthePVCresin.1.1Thistestmethodissuitablefordeterminingtheresidualvinylchloridemonomer(RVCM)contentofpoly(vinylchloride)(PVC)homopolymerandcopolymerresinsforusesotherthanfoodcontact.Therangeforthistest,basedoninterlaboratoryevaluation,isfrom0.1to400ppmRVCM.1.2ThistestmethodcanbeadaptedtodeterminationsofRVCMinaPVCcopolymerresiniftheHenry''sLawconstantat90x00B0;Cforthatcopolymerisknown.1.3Thistestmethodcannotbeusedforpolymerinfusedforms,suchascubesorsheets.RefertoTestMethodD4443orTestMethodD3680forthesematerials.1.4ThistestmethodisproposedasanalternativetoEPAMethod107fordeterminationofvinylchloridemonomersindry-resinsamples.1.5ThevaluesstatedSIunitsaretoberegardedasthestandard.1.6Thisstandarddoesnotpurporttoaddressallofthesafetyconcerns,ifany,associatedwithitsuse.Itistheresponsibilityoftheuserofthisstandardtoestablishappropriatesafetyandhealthpracticesanddeterminetheapplicabilityofregulatorylimitationspriortouse.Note18212;ThisstandardandISO6401:2008addressthesamesubjectmatter,butdifferintechnicalcontent.
【中国标准分类号】:G31
【国际标准分类号】:83_080_20
【页数】:4P.;A4
【正文语种】:英语
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